Química Nova

URI permanente para esta coleçãohttps://thoth.dti.ufv.br/handle/123456789/13323

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2009 - 200912010 - 20121

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Autor: search.filters.author.Bandeira, Raquel D. C. C.Tem arquivos: Sim

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    Development and validation of a method for the analysis of ochratoxin a in roasted coffee by liquid chromatography/electrospray-mass spectrometry in tandem (LC/ESI-MS/MS)
    (Sociedade Brasileira de Química, 2012) Bandeira, Raquel D. C. C.; Uekane, Thais M.; Cunha, Carolina P. da; Geaquinto, Luths R. O.; Cunha, Valnei S.; Caixeiro, Janaina M. R.; Godoy, Ronoel Luiz O.; Cruz, Marcus Henrique C. de la
    A method using LC/ESI-MS/MS for the quantitative analysis of Ochratoxin A in roasted coffee was described. Linearity was demonstrated (r = 0.9175). The limits of detection and quantification were 1.0 and 3.0 ng g-1, respectively. Trueness, repeatability and intermediate precision values were 89.0-108.8%; 2.4-13.7%; 12.5-17.8%, respectively. To the best of our knowledge, this is the first report in which Ochratoxin A in roasted coffee is analysed by LC/ESI-MS/MS, contributing to the field of mycotoxin analysis, and it will be used for future production of Certified Reference Material.
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    Composição volátil dos defeitos intrínsecos do café por CG/EM-headspace
    (Sociedade Brasileira de Química, 2009) Bandeira, Raquel D. C. C.; Toci, Aline T.; Trugo, Luiz C.; Farah, Adriana
    About 20% of Brazilian raw coffee production is considered inappropriate for exportation. Consequently, these beans are incorporated to good quality beans in the Brazilian market. This by-product of coffee industry is called PVA due to the presence of black (P), green (V) and sour (A) defective beans which are known to contribute considerably for cup quality decrease. Data on the volatile composition of Brazilian defective coffee beans are scarce. In this study, we evaluated the volatile composition of immature, black-immature, black defective beans and PVA compared to good quality beans. Potential defective beans markers were identified.