Brazilian Journal of Food Technology
URI permanente para esta coleçãohttps://thoth.dti.ufv.br/handle/123456789/13098
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Item Variability of volatile compound profiles during two coffee fermentation times in northern Peru using SPME-GC/MS(Instituto de Tecnologia de Alimentos – ITAL, 2023-05-15) Perez, Jhordy; Calderon, Martha Steffany; Bustamante, Danilo Edson; Caetano, Aline Camila; Mendoza, Jani Elisabet; Fernandez-Güimac, Samia Littly JahavelyThe time of the fermentation process of coffee from northern Peru is variable (9 to 48 hours) since coffee farmers do not use standardized processes, causing a variety of coffee qualities. This study aimed to identify volatile compounds in both short (9 hours) and long (32 hours) coffee fermentation processes from coffee farms in northern Peru using Solid-Phase Microextraction-Gas Chromatography/Mass Spectrometry (SPME-GC/MS) to associate the coffee quality and diversity of volatile compounds. Sensory analyses showed that the short fermentation process (SFP) scored 77.8 ± 0.39 and had chocolate, wood, cardboard, dry, fatty and rough notes, while the long fermentation process (LFP) showed higher punctuations 85.5 ± 3.16 and citrus, fruity, floral, caramel and chocolate sensory attributes. A total of 90 compounds were found in the SFP, whereas 141 compounds were identified in the LFP. Significant differences in the relative abundance of 14 chemical compounds were reported in the SFP and LFP (p < 0.05). From these results, the presence of benzaldehyde, methional, hexanal, 2-heptanone, pentadecane, 1-butanol-3-methyl-acetate, and benzene-acetic acid ethyl ester seems to impact the quality of coffee. The analysis of similarities showed that coffee samples (5 h and 9 h) during the SFP were very variable, whereas coffee samples from LFP showed some tendency to group, which may be related to the difference in altitude and temperature in coffee farms making comparison between them difficult. In addition, this study highlights the complex relationship between coffee fermentation and flavour and the influence of several factors and variables that may affect the composition of flavour and aroma precursors in green coffee beans obtained from wet fermentation.Item Arabica coffee flow properties assessed using different roasts and particle sizes during storage(Instituto de Tecnologia de Alimentos – ITAL, 2022-02-18) Oliveira, Gabriel Henrique Horta de; Corrêa, Paulo Cesar; Oliveira, Ana Paula Lelis Rodrigues de; Vargas-Elías, Guillermo Asdrúbal; Calil Júnior, CarlitoFlowability of agricultural products is an important factor to be considered at post-harvest, thus impacting directly on number of operations and the design of machinery. This study aimed to evaluate and determine the K coefficient and flow properties as a function of different levels of roasting, grain size, temperature and storage. Coffee beans were roasted at medium light and moderately dark, then ground at fine, medium and coarse sizes. An additional coffee lot was not ground. Samples were stored at 10 ºC and 30 ºC and analyzed during storage (0, 30, 60, 120 and 180 days), regarding internal and external friction coefficients, angle of internal friction, effective angle of internal friction, wall friction angle (concrete, rough steel and wood) and lateral pressure coefficient (K coefficient). Angle of internal friction varied significantly due to particle size and roast degree. Moderately dark roast with fine particle size led to higher values (about 29.5 º) of wall friction angle. The wood sample was the material with the highest values of wall friction angle, followed by the concrete and steel samples, when compared at the same storage temperature, roast degree and particle size. Whole coffee was classified as free-flowing. Fine particle size leads to cohesive flow characteristic, according to the flow function. Coffee roasted at medium light, kept whole requires storage facilities with higher pressure support, accordingly to the K coefficient values.Item Modeling and simulation of heat and mass transfer during drying of coffee in a box dryer using C++ programming language(Instituto de Tecnologia de Alimentos – ITAL, 2021) Rabello, Gildeir Lima; Pimentel, Uilla Fava; Aranda, Donato; Poubel, WillianDrying is one of the stages of coffee processing and has been considered one of the factors that impact the quality of the final drink. In this sense, the present study developed a phenomenological model for a box-type dryer implementing in C / C ++ programming language. The profile of the exhaust air temperature was obtained over the drying time. The model was verified by comparing data obtained from the literature, thus guaranteeing its functionality to make predictions about the air temperature profile in equipment used by small coffee producers, which may contribute to the increase in product quality.Item Properties of dark chocolate enriched with free and encapsulated chlorogenic acids extracted from green coffee(Instituto de Tecnologia de Alimentos – ITAL, 2020) Zohreh, DidarTo increase the functionality of dark chocolate, chlorogenic acids extracted from green coffee were added in free or encapsulated forms at different concentration (10, 20, 30, 40 and 50 mg/5 kg of free chlorogenic acids and equal quantity of encapsulated form). The extraction of chlorogenic acids was carried out by maceration of ground green coffee beans in distilled water (30 min at 80 °C), then, cooling, filtration and adsorption by active carbon were done. The final step was filtration and desorption from active carbon and rotary drying (at 60 °C and 120 rpm). Encapsulation of chlorogenic acids was done by coacervation of pectin and gelatin. For quality assessment, several analysis on chocolate samples were performed included color index and melting behavior by Differential Scanning Calorimeter. Flow behavior of the chocolate samples melted at 40 °C was determined using stress or strain controlled rheometer. The microstructure of the chocolate samples was analyzed by Scanning Electron Microscope technique at 500-1000x magnification. Particle size distribution and sensory evaluation was also performed. Results showed addition of free and encapsulated forms of chlorogenic acids decreased Tonset, Tpeak and ΔH of dark chocolate. Casson viscosity increased in the case of addition chlorogenic acids. Color indexes of chocolate samples were influenced by addition of chlorogenic acids. Particle size distribution decreased with addition of free form and increased when encapsulated form was added. Sensory characteristics were also influenced by chocolate formulation and samples included encapsulated chlorogenic acids exhibit better sensory properties than samples enriched with free form.Item Otimização por Page do processo de secagem em leito de espuma para produção de café solúvel(Instituto de Tecnologia de Alimentos – ITAL, 2020) Silva, Gustavo Henrique Souza; Bressani, Ana Paula Pereira; Junqueira, Mateus da SilvaA expansão da produção de café solúvel é uma alternativa ao consumo do café tradicional, tornando-se necessária para atender às novas exigências dos consumidores que buscam conveniência e praticidade. Diante desse cenário, o estudo de técnicas que simplificam e reduzem custos para a obtenção de café solúvel se torna mais pertinente. Portanto, o objetivo deste trabalho foi otimizar o processo de secagem de extrato de café em leito de espuma, por meio do ajuste ao Modelo de Page por regressão não linear. Foram avaliados dois métodos para a concentração do extrato: (A) em evaporador rotativo e (B) em recipiente de inox aberto. A cinética de secagem do extrato de café em leito de espuma sob as temperaturas de 40, 50, 60, 70 e 80 °C foi descrita pelo modelo. Além disso, foi proposta uma equação multivariada para a secagem mediante detecção da influência da temperatura no parâmetro k, do Modelo de Page, e posterior validação dos resultados. O tempo para obtenção do extrato concentrado foi próximo para os dois métodos de concentração (A: 2 horas e 30 minutos; B: 2 horas e 40 minutos). O modelo de Page apresentou ótimo ajuste com valores de coeficientes de determinação acima de 99%. Por meio dos resultados obtidos, foi confirmado que a temperatura é um fator determinante na velocidade de perda de umidade do produto, apresentando tempos de secagem menores com o aumento da temperatura. A correlação entre os dados experimentais e preditos foi satisfatória para validar os resultados. O modelo matemático também pode auxiliar na correlação dos parâmetros de secagem com alterações físico-químicas e sensoriais do café solúvel, a fim de melhorar os parâmetros tecnológicos.